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05925nam a2200709 a 4500 |
| 001 - CONTROL NUMBER |
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EBC954643 |
| 003 - CONTROL NUMBER IDENTIFIER |
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MiAaPQ |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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20180702100642.0 |
| 007 - PHYSICAL DESCRIPTION FIXED FIELD--GENERAL INFORMATION |
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cr cn |||m|||a |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
120913s2012 nyua foab 001 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
9781606503522 (electronic bk.) |
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| International Standard Book Number |
1606503529 (electronic bk.) |
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| Cancelled/invalid ISBN |
9781606503508 (print) |
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| Cancelled/invalid ISBN |
1606503502 (print) |
| 024 7# - OTHER STANDARD IDENTIFIER |
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| Standard number or code |
10.5643/9781606503522 |
| Source of number or code |
doi |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(OCoLC)809804677 |
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| System control number |
(CaBNvSL)swl00401257 |
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| System control number |
(MiAaPQ)EBC954643 |
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| System control number |
(Au-PeEL)EBL954643 |
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| System control number |
(CaPaEBR)ebr10588196 |
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| System control number |
(CaONFJC)MIL420849 |
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| System control number |
(OCoLC)830170650 |
| 040 ## - CATALOGING SOURCE |
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| Original cataloging agency |
MiAaPQ |
| Transcribing agency |
MiAaPQ |
| Modifying agency |
MiAaPQ |
| 050 #4 - LIBRARY OF CONGRESS CALL NUMBER |
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| Classification number |
QD96.N8 |
| Item number |
A668 2012 |
| 082 04 - DEWEY DECIMAL CLASSIFICATION NUMBER |
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| Classification number |
543.0877 |
| Edition number |
23 |
| 100 1# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Apperley, David C. |
| 245 10 - TITLE STATEMENT |
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| Title |
Solid-state NMR |
| Medium |
[electronic resource] : |
| Remainder of title |
basic principles & practice / |
| Statement of responsibility, etc |
David C. Apperley, Robin K. Harris & Paul Hodgkinson. |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT) |
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| Place of publication, distribution, etc |
[New York, N.Y.] (222 East 46th Street, New York, NY 10017) : |
| Name of publisher, distributor, etc |
Momentum Press, |
| Date of publication, distribution, etc |
2012. |
| 300 ## - PHYSICAL DESCRIPTION |
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| Extent |
1 electronic text (xiv, 276 p.) : |
| Other physical details |
ill., digital file. |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
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| Bibliography, etc |
Includes bibliographical references and index. |
| 505 0# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
Preface -- About the authors -- |
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| Formatted contents note |
1. Introduction -- 1.1 The utility of NMR -- 1.2 A preview of solid-state NMR spectra -- 1.3 The solid state -- 1.4 Polymorphism, solvates, co-crystals & host:guest systems -- 1.5 NMR of solids & the periodic table -- |
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| Formatted contents note |
2. Basic NMR concepts for solids -- 2.1 Nuclear spin magnetization -- 2.2 Tensors -- 2.3 Shielding -- 2.4 Indirect coupling -- 2.5 Dipolar coupling -- 2.6 Quadrupolar coupling -- 2.7 Magic-angle spinning -- 2.8 Relaxation -- |
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| Formatted contents note |
3. Spin-1/2 nuclei: a practical guide -- 3.1 Introduction -- 3.2 The vector model & the rotating frame of reference -- 3.3 The components of an NMR experiment -- 3.4 Cross polarization -- 3.5 High-resolution spectra from 1H (& 19F) -- |
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| Formatted contents note |
4. Quantum mechanics of solid-state NMR -- 4.1 Introduction -- 4.2 The Hamiltonians of NMR -- 4.3 The density matrix -- 4.4 Density operator treatments of simple NMR experiments -- 4.5 The density matrix for coupled spins -- 4.6 Euler angles & spherical tensors -- 4.7 Additional analytical tools -- |
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| Formatted contents note |
5. Going further with spin-1/2 solid-state NMR -- 5.1 Introduction -- 5.2 Linewidths in solid-state NMR -- 5.3 Exploiting indirect (J) couplings in solids -- 5.4 Spectral correlation experiments -- 5.5 Homonuclear decoupling -- 5.6 Using correlation experiments for spectral assignment -- 5.7 Further applications -- |
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| Formatted contents note |
6. Quadrupolar nuclei -- 6.1 Introduction -- 6.2 Characteristics of first-order quadrupolar spectra -- 6.3 First-order energy levels & spectra -- 6.4 Second-order zero-asymmetry cases -- 6.5 Spectra for cases with non-zero asymmetry: central transition -- 6.6 Recording one-dimensional spectra of quadrupolar nuclei -- 6.7 Manipulating the quadrupolar effect -- 6.8 Spectra for integral spins -- |
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| Formatted contents note |
7. Relaxation, exchange & quantitation -- 7.1 Introduction -- 7.2 Relaxation -- 7.3 Exchange -- 7.4 Quantitative NMR -- 7.5 Paramagnetic systems -- |
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| Formatted contents note |
8. Analysis & interpretation -- 8.1 Introduction -- 8.2 Quantitative measurement of anisotropies -- 8.3 Measurement of dipolar couplings -- 8.4 Quantifying indirect (J) couplings -- 8.5 Tensor interplay -- 8.6 Effects of quadrupolar nuclei on spin-1/2 spectra -- 8.7 Quantifying relationships between tensors -- 8.8 NMR crystallography -- |
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| Formatted contents note |
Appendices -- A. The spin properties of spin-1/2 nuclides -- B. The spin properties of quadrupolar nuclides -- C. Liouville space, relaxation & exchange -- C.1 Introduction to Liouville space -- C.2 Application to relaxation -- C.3 Application to chemical exchange -- D. Introduction to solid-state NMR simulation -- D.1 Specifying the spin system -- D.2 Specifying the powder sampling -- D.3 Specifying the pulse sequence -- D.4 Efficiency of calculation -- Index. |
| 506 ## - RESTRICTIONS ON ACCESS NOTE |
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| Terms governing access |
Restricted to libraries which purchase an unrestricted PDF download via an IP. |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc |
Nuclear magnetic resonance (NMR) has proved to be a uniquely powerful and versatile spectroscopy, and no modern university chemistry department or industrial chemistry laboratory is complete without a suite of NMR spectrometers. The phenomenon of nuclear spin may seem an odd basis for an analytical tool, but it is the relative isolation of the nuclear spin from its surroundings that makes it an ideal noninterfering probe of the electronic environment. Different sites are clearly identified by their chemical shifts, while J couplings in 1H spectra provide connectivity information. The combination of these two complementary interactions, plus the formidable array of different NMR experiments developed since the arrival of Fourier transform NMR in 1966, has revolutionized the practice of chemistry. |
| 530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE |
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| Additional physical form available note |
Also available in print. |
| 533 ## - REPRODUCTION NOTE |
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| Type of reproduction |
Electronic reproduction. Ann Arbor, MI : ProQuest, 2015. Available via World Wide Web. Access may be limited to ProQuest affiliated libraries. |
| 538 ## - SYSTEM DETAILS NOTE |
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| System details note |
Mode of access: World Wide Web. |
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| System details note |
System requirements: Adobe Acrobat reader. |
| 588 ## - |
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| -- |
Title from PDF t.p. (viewed on September 13, 2012). |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name as entry element |
Nuclear magnetic resonance spectroscopy. |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
Solid-state NMR |
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| Uncontrolled term |
Magic-angle spinning |
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| Uncontrolled term |
Solid-state structure |
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| Uncontrolled term |
NMR crystallography |
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| Uncontrolled term |
Cross polarization |
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| Uncontrolled term |
Quadrupolar nuclei |
| 655 #4 - INDEX TERM--GENRE/FORM |
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| Genre/form data or focus term |
Electronic books. |
| 700 1# - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Harris, Robin K. |
| Fuller form of name |
(Robin Kingsley) |
|
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| Personal name |
Hodgkinson, Paul. |
| 776 08 - ADDITIONAL PHYSICAL FORM ENTRY |
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| Display text |
Print version: |
| International Standard Book Number |
1606503502 |
| -- |
9781606503508 |
| 856 40 - ELECTRONIC LOCATION AND ACCESS |
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| Uniform Resource Identifier |
https://ebookcentral.proquest.com/lib/kliuc-ebooks/detail.action?docID=954643 |
| Public note |
Click to View |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
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| Source of classification or shelving scheme |
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| Koha item type |
E-book |
